Laboratoire de chimie de la matière condensée de Paris
Tour 44-43 / 4ème étage
Case courrier 174
4, Place Jussieu
75005 PARIS
France

Pr. Christian BONHOMME

Professeur
SMiLES

christian.bonhomme(@-Code a retirer pour éviter le SPAM-)sorbonne-universite.fr

Christian Bonhomme is a chemical engineer from the Ecole Nationale Supérieure de Chimie de Paris (ENSCP) and graduated in 1990. He defended his doctoral thesis in 1994 under the supervision of Pr J. Livage. During the last year of his thesis he was interested more particularly in solid state NMR methods and in cross-polarization under fast MAS, then a central topic in the NMR community. Assistant Professor in 1994, he spent his entire career at the Laboratoire de Chimie de la Matière Condensée de Paris (LCMCP) at Sorbonne University, Paris, France. He is currently full Professor (exceptionnal class 2 – highest level in France). From 2009 to 2011 he was Visiting Professor at the Physics Department of the University of Warwick, UK (SOME REFS). He has established a very strong collaboration with several English colleagues and is a regular user of the NMR UK national facility [ref]. He has established numerous national and international collaborations: TO COMPLETE (people + 1 ref…).

He has presented §§ invited national and international conferences, most recently PANACEA (September 2024, Aveiro, Portugal), §§§§. Lectures cover both solid state NMR and DNP applied to the study of materials, and mathematical developments related to spin dynamics and associated numerical methods. Among §§§ articles and abstracts, he is the author of §§ reviews in NMR applications in materials science [Accounts Chem Res 2007-Progress NMR 2014-SSNMR 2020], DFT calculations of NMR parameters [Chem rev 2012-Book 2014] and data treatment [GUL].

Currently, his scientific topics of interest are: (1) NMR/DNP [1-2-3] including methodology for non-sensitive nuclei such as ⁴³Ca and ¹⁷O [2017+…]; (2) Instrumentation & signal processing [4-5]; (3) DFT, ab initio calculations of NMR parameters, NMR crystallography & MD simulations [6-7,8]; (4) Applications in materials science including synthetic [§§] and natural biomaterials such as pathological calcifications (kidney stones) [9-10]; (5) Precipitation in confined media [§§§]; (6) Graph theory & Path-Sum for Quantum Mechanics/spin dynamics in NMR/DNP [11].

During the first years of his career, he trained himself in the theoretical aspects of solid-state NMR and was able to propose in 1998 an original mathematical description of the macroscopic reorientations of the sample in NMR, generalizing to upper ranks the ellipsoid representation traditionally used in physics for the description of rank 2 tensors [12-13-14]. In his HDR (Habilitation à Diriger des Recherches) defended in 2003, he proposes in conclusion to include Feynman paths in spin dynamics. He concretizes this proposal in 2020 [11] in very close collaboration with P.-L. Giscard, mathematician at Université du Littoral Côte d’Opale, Calais, France. In this context, he is also working with S. Pozza – a specialist in matrix calculus at Charles University, Prague, Czech Republic, on ultra-fast codes for solving systems of coupled linear differential equations (related to spin dynamics) [§§].

[1] C. Bonhomme, C. Gervais, D. Laurencin, Prog. Nucl. Magn. Reson. Spectr., 77, 1-48 (2014). [2] C. Leroy, F. Aussenac, L. Bonhomme-Coury, A. Osaka, S. Hayakawa, F. Babonneau, C. Coelho-Diogo, C. Bonhomme, Analytical Chem., 89, 10201-10207 (2017). [3] D. Lee, C. Leroy, C. Crevant, L. Bonhomme-Coury, F. Babonneau, D. Laurencin, C. Bonhomme, G. De Paëpe, Nature Commun., 8, 14104 (2017). [4] A. Lehmann-Horn, J.-F. Jacquinot, J. C. Ginefri, C. Bonhomme, D. Sakellariou, J. Magn. Reson., 271, 46‑51 (2016). [5] G. Laurent, W. Woelffel, V. Barret-Vivin, E. Gouillart, and C. Bonhomme, Appl. Spectrosc. Rev., 54, 602-630 (2019). [6] C. Bonhomme, C. Gervais, C. Coelho, F. Pourpoint, T. Azaïs, F. Babonneau, S. Ashbrook, J. Griffin, J. Yates, C. J. Pickard, F. Mauri, Chemical Reviews, 112, 5733-5779 (2012). [7] C. Bonhomme, C. Gervais, N. Folliet, F. Pourpoint, C. Coelho-Diogo, J. Lao, E. Jallot, J. Lacroix, J.M. Nedelec, D. Iuga, J.V. Hanna, M.E. Smith, Y. Xiang, J. Du, D. Laurencin, J. Am. Chem. Soc., 134(30), 12611‑12628 (2012). [8] C. Bonhomme, X.L. Wang, I. Hung, Z.H. Gan, C. Gervais, C .Sassoye, J. Rimsza, J.C. Du, M.E. Smith, J.V. Hanna, S. Sarda, P. Gras, C. Combes, D. Laurencin, Chemical Commun. 54, 9591‑9594 (2018). [9] L. Mayen, N. D. Jensen, D. Laurencin, O. Marsan, C. Bonhomme, C. Gervais, M. E. Smith, C. Coelho, G. Laurent, J. Trebosc, Z. Gan, K. Chen, C. Rey, C. Combes, J. Soulie, Acta Biomaterialia, 103, 333-345 (2020). [10] C. Gervais, C. Bonhomme, D. Laurencin, Solid State NMR, 2020, 107:101663. [11] P.‑L. Giscard, C. Bonhomme, Phys. Rev. Res., 2, 023081 (2020). [12] C. Bonhomme, J. Livage, J. Phys. Chem. A, 103, 460-477 (1999). [13] C. Bonhomme, J. Livage, J. Phys. Chem. A, 102, 375-385 (1998). [13] C. Bonhomme, T. Azaïs, C.R. Chimie, 7, 417-424 (2004).

1- Towards an « Infinite » Number of Calcium Oxalate Structures? (IUCr, 2023, Melbourne, Australia) – KEYNOTE speaker

2- Path-Sum: a New Avenue for Spin Dynamics (43rd FGMR Annual Discussion Meeting, 2022) – PLENARY speaker

3- New Potentialities of NMR and DNP for the Study of Biomaterials: Experiments and Theory (Experimental Nuclear Magnetic Resonance Conference, 2022) – INVITED speaker

Solid state NMR

CP dynamics including Inversion Recovery Cross Polarization (IRCP) is an invaluable tool of investigation for the detailed study of local dynamics (Chem. Mater. 1996, 8, 1415-1428) including unexpected molecular reorientation « at the Magic Angle » in some silsesquioxanes (J. Chem. Soc. Dalton Trans. 1997, 1617-1626; J. Am. Chem. Soc. 1998, 120, 8380-8391) and distance measurements in multiple-spin systems (Solid State NMR 2005, 28, 50-56). Halogen NMR such as ³⁵Cl at various (high) magnetic fields is a useful spectroscopic probe for OH…Cl hydrogen bond in static and (moderate) MAS modes (Solid State NMR 2003, 23, 14-27).

Solid state NMR methodology is developed in the framework of J-derived techniques under fast MAS in connection with the first principles calculations of J couplings by GIPAW (Inorg. Chem. 2007, 46, 1379‑1387; Accounts Chem. Res. 2007, 40, 738-746), exotic non sensitive nuclei such ⁴³Ca and ⁸⁷Sr (J. Am. Chem. Soc. 2009, 131, 13430-13440; J. Am. Chem. Soc. 2012, 134, 12611-12628), ultra-broad spectra (ChemistrySelect 2016, 4509-4519) and ultra-high magnetic field: 35.1 T, 1.5 GHz (Chem. Commun. 2018, 69, 9591-9594).

A/ Ultra-high resolution ⁴³Ca MAS spectra for calcium pyrophosphates and oxalate obtained at ultra-high magnetic field (35.1 T, 1.5 GHz) at NHMFL, Tallahassee, FL, USA. Dashed lines correspond to GIPAW calculations. Adapted from Chem. Commun. **2018**, 69, 9591-9594. B/ ¹H-¹³C-⁴³Ca TRADOR experiments related to tri-hydrated calcium benzoate *Ca(C₆H₅COO)₂.3H₂O at 9.4 T, 400 MHz, partially labeled in ⁴³Ca. Adapted from J. Am. Chem. Soc. **2009**, 131, 13430-13440.

DNP (Dynamic Nuclear Polarization)

DNP has revolutionalized the description of carbonated hydroxyapatite (Analytical Chem. 2017, 89, 10201-10207). ¹H-¹H spin diffusion is quasi one-dimensional along the OH^– columns (parallel to the c-axis). Local order and clustering of the carbonate anions is clearly demonstrated by ¹³C-¹³C homonuclear correlation MAS DNP experiments. The clusters of carbonates are located in zig-zag chains along the c-axis of the structure. The DNP enhancement is sufficient to implement ¹H-⁴³Ca HETCOR experiments in natural abundance which is a true challenge for this nucleus (0.14% and low gamma) (Nature Commun. 2017, 8, 14104).

A/ Schematic representation of the hydroxyapatite structure partially substituted by carbonate anions (black triangle in the OH^– column). During DNP, the protons at the surface of the nanoparticles are first hyperpolarized. Then the polarization is transported by spin diffusion along the columns in a quasi one-dimensional process. Adapted from Analytical Chem. **2017**, 89, 10201-10207. B/ The first ¹H-⁴³Ca HETCOR CP MAS DNP experiment in natural abundance (⁴³Ca: 0.14%) obtained in 4 hours. Adapted from Nature Commun. **2017**, 8, 14104.

Instrumentation

Sensitivity remains the main drawback of NMR. Following Sakellariou et al., MACS (Magic Angle Coil Spinning) is a perfect alternative for samples characterized by a low mass (such as biological samples). The solenoid geometry for the microcoil is among the most versatile ones, is suitable for microfabrication (PLOS ONE 2012, 7, e42848) reaching an enhancement of 5-10 in certain cases. Recently, monolithic MACS microresonators were developed for high resolution NMR keeping intact the intrinsic cylindrical symmetry of the set-up and allowing for fast MAS (J. Magn .Reson. 2016, 271, 46-51).

A/ Magic Angle Coil SPinning (MACS) concept developed by Sakellariou et al. Microfabricated solenoid microcoils. Adapted from PLOS ONE **2012**, 7, e42848. B/ Monolithic MACS resonators used for MACS applications. Adapted from J. Magn. Reson. 2016, 271, 46-51.

Signal processing

Major improvement has been obtained in the denoising of time-domain signal by using Singular Value Decomposition (SVD) accelarated by Graphics Processing Units (GPU) (Solid State NMR 2014, 61-62, 28-34). (J. Magn .Reson. 2016, 271, 46-51). SVD limits have been deeply investigated recently (Appl. Spectr. Rev. 2019, 54, 602-630). A 100 gain in time was achieved by combining divide and conquer algorithm, Intel Math Kernel Library (MKL), SSE3 (Streaming SIMD Extensions) hardware instructions and single precision. In such case, the CPU can outperform the GPU driven by CUDA technology. (Appl. Spectr. Rev. 2020, 55, 173-196).

A/ Denoising (Cadzow) procedure. Hankel matrix H contains the digitised noisy time-domain signal. Σ_1,2,3correspond to the singular values. Adapted from Solid State NMR **2014**, 61-62, 28-34. B/ Influence of the number of columns (n) for Toeplitz FID matrix construction for a ²⁹Si CPMG solid state NMR spectrum of 50/50 MTEOS/TEOS (CH₃Si(OEt)₃/Si(OEt)₄) sample. Adapted from Appl. Spectr. Rev. **2019**, 54, 602-630.

First principles calculations of NMR parameters, NMR crystallography

Following the pionneering work of Pickard and Mauri (2001), first principles calculations of NMR parameters were systematically implemented in the case of molecular inorganic (Magn. Res .Chem. 2004, 42, 445-452; J. Am. Chem. Soc. 2010, 132, 4653-4668; J. Am. Chem. Soc. 2012, 134, 12611-12628) and organic solids (J. Phys. Chem. A 2005, 109, 6960-6969), biocompatible materials (App. Magn. Res. 2007, 32, 435-457; CrystEngComm 2013, 15, 8840-8847; Acta Biomater. 2016, 31, 348-357), molecular dynamics (Phys. Chem. Chem. Phys. 2009, 11, 6953-6961) and non crystalline solids (J. Am. Chem. Soc. 2012, 134, 12611-12628; Chem. Commun. 2018, 54, 9591-9594). For a review article: Chem. Reviews 2012, 112, 5733-5779.

A/ MD simulations of amorphous calcium pyrophosphate glasses (a-CPP) for various level of hydration (n), ⁴³Ca MAS NMR spectrum at ultra-high magnetic field (35.1 T) and associated ⁴³Ca isotropic chemical shifts calculated by GIPAW. Adapted from Chem. Commun **2018**, 54, 9591-9594. B/ Correlation between the computed ⁴³Ca isotropic chemical shifts and the mean Ca. . .O bond distance in various calcium pyrophosphates, depending on the Ca coordination number (CN) and the number of water molecules in the coordination sphere. Adapted from Acta Biomater. **2016**, 31, 348-357.

Applications in materials science

We focus here on our latest interest in soft-chemistry applied to the systhesis of amorphous calcium ortho/pyrophosphate biomaterials of tunable composition (Acta Biomater. 2020, 103, 333-345) and more generally to advanced NMR methods applied to the characterization of biocompatible materials (Solid State NMR, 2020, 107:101663).

A/ ³¹P SQ-DQ spectrum of ortho/pyrophosphate glass acquired at 16.4 T, spinning at 14 kHz. The dashed red boxes show the cross-peaks between ortho and pyrophosphate units. B/ ²³Na-³¹ P D-HMQC spectrum (heteronuclear dipolar correlation) of ortho/pyrophosphate glass, acquired at 18.8 T using 20 kHz spinning speed (the ²³Na NMR spectra in blue and red correspond to correlations with pyro- and orthophosphate ions, respectively). Adapted from Acta Biomater. **2020**, 103, 333-345.

Quantum mechanics and Path-Sum

In collaboration with P.-L. Giscard, we have applied the Path-Sum concept to NMR for the first time solving analytically the Bloch-Siegert effect at all order (avoiding perturbative treatments), spin diffusion in an organimetallic molecule exhibiting 42 protons and giving entirely new insight in Coherent Destruction of Tuneling, CDT (ENC 2019, Asilomar, USA; Phys. Rev. Res., 2020, 2, 023081). We recently solved the Bloch equations in their most general form (ENC 2020, Baltimore, Zoom conference, USA).

A/ The dynamical graph associated to the time-dependent matrix A(t). Adapted from ENC, **2019**, Asilomar, USA. B/ Path-Sum applied to Bloch-Siegert effect from weak- to ultra-strong coupling. Adapted from Phys. Rev. Res. **2020**, 2, 023081.

Solid state NMR (Master, Sorbonne University)
Solid state NMR tutorials (Master, Sorbonne University)
NMR exams (Master, Sorbonne University)
Characterization of biological materials (Master, Sorbonne University)
Silicon: from periodic table to biogenic silica (BSc, Sorbonne University)
Zeolites and porous structures (BSc, Sorbonne University)
Introduction to spectroscopy (BSc, Sorbonne University)
Introduction to thermal analyses (BSc, Sorbonne University)

Starting in 1946

DNP/NMR @ LCMCP: instrumentation, beyond standard GIPAW and applications to biomaterials (4^th sino-french workshop, 2017, Wuhan, China)
Solid state NMR: new trends in materials science (2^nd Edition of the International Summer School Physical and Chemical Principles in Materials Science, 2016, Paris, France)
Principes de base en Résonance Magnétique Nucléaire (Ecole thématique Magnétisme et Résonances Magnétiques : Outils et Applications, 2015, Autrans, France,).

Journal articles

ref_biblio: Adam Nelson, Wassilios Papawassiliou, Subhradip Paul, Sabine Hediger, Ivan Hung, et al.. Temperature-induced mobility in octacalcium phosphate impacts crystal symmetry: water dynamics studied by NMR crystallography. Faraday Discussions, 2025, 255, pp.451-482. ⟨10.1039/D4FD00108G⟩. ⟨hal-04930142⟩
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ref_biblio: Ieva Goldberga, Ivan Hung, Vincent Sarou-Kanian, Christel Gervais, Zhehong Gan, et al.. High-Resolution 17 O Solid-State NMR as a Unique Probe for Investigating Oxalate Binding Modes in Materials: The Case Study of Calcium Oxalate Biominerals. Inorganic Chemistry, 2024, 63 (22), pp.10179-10193. ⟨10.1021/acs.inorgchem.4c00300⟩. ⟨hal-04603458⟩
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ref_biblio: Yangyang Su, Flavio Siro Brigiano, Ivan Petit, César Leroy, Christian Bonhomme, et al.. Investigation of Carbonate Substitution in Hydroxyapatite by Combining Solid‐state NMR and DFT Calculations. Chemistry–Methods, 2023, ⟨10.1002/cmtd.202300007⟩. ⟨hal-04138043⟩
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ref_biblio: Vinicius Martins, Bryan E.G. Lucier, Kuizhi Chen, Ivan Hung, Zhehong Gan, et al.. Molecular-Level Characterization of Oxygen Local Environments in a Pristine and Post-Synthetically Modified Metal–Organic Framework via 17 O Nuclear Magnetic Resonance Spectroscopy. Chemistry of Materials, 2023, 35 (9), pp.3555-3569. ⟨10.1021/acs.chemmater.3c00199⟩. ⟨hal-04137974⟩
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ref_biblio: Ieva Goldberga, Nicholai D Jensen, Christèle Combes, Frédéric Mentink-Vigier, Xiaoling Wang, et al.. 17O solid state NMR as a valuable tool for deciphering reaction mechanisms in mechanochemistry: the case study on the 17 O-enrichment of hydrated Ca-pyrophosphate biominerals. Faraday Discussions, 2023, 241, pp.250-265. ⟨10.1039/d2fd00127f⟩. ⟨hal-03846476⟩
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ref_biblio: Ieva Goldberga, Nicolas Patris, Chia-Hsin Chen, Emilie Thomassot, Julien Trébosc, et al.. First Direct Insight into the Local Environment and Dynamics of Water Molecules in the Whewellite Mineral Phase: Mechanochemical Isotopic Enrichment and High-Resolution ¹⁷O and ²H NMR Analyses. Journal of Physical Chemistry C, 2022, 126 (29), pp.12044 - 12059. ⟨10.1021/acs.jpcc.2c02070⟩. ⟨hal-03741471⟩
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ref_biblio: Vinicius Martins, Jun Xu, Ivan Hung, Zhehong Gan, Christel Gervais, et al.. 17 O solid‐state NMR at ultrahigh magnetic field of 35.2 T: Resolution of inequivalent oxygen sites in different phases of MOF MIL‐53(Al). Magnetic Resonance in Chemistry, 2021, 59 (9-10), pp.940-950. ⟨10.1002/mrc.5122⟩. ⟨hal-03572397⟩
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ref_biblio: César Leroy, Laure Bonhomme-Coury, Christel Gervais, Frederik Tielens, Florence Babonneau, et al.. A novel multinuclear solid state NMR approach for the characterization of kidney stones. Magnetic Resonance, 2021, 2 (2), pp.653-671. ⟨10.5194/mr-2-653-2021⟩. ⟨hal-03322334v2⟩
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ref_biblio: Danielle Laurencin, Yang Li, Melinda J Duer, Dinu Iuga, Christel Gervais, et al.. A 43 Ca NMR perspective on octacalcium phosphate and its hybrid derivatives. Magnetic Resonance in Chemistry, 2021, 59, pp.1048. ⟨10.1002/mrc.5149⟩. ⟨hal-03177548⟩
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ref_biblio: Vinicius Martins, Jun (jim) Xu, Xiaoling Wang, Kuizhi Chen, Ivan Hung, et al.. Higher Magnetic Fields, Finer MOF Structural Information: 17 O Solid-State NMR at 35.2 T. Journal of the American Chemical Society, 2020, 142 (35), pp.14877-14889. ⟨10.1021/jacs.0c02810⟩. ⟨hal-02925283⟩
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ref_biblio: Theau Debroise, Thomas Sedzik, Jelle Vekeman, Yangyang Su, Christian Bonhomme, et al.. Morphology of Calcium Oxalate Polyhydrates: A Quantum Chemical and Computational Study. Crystal Growth & Design, 2020, 20 (6), pp.3807-3815. ⟨10.1021/acs.cgd.0c00119⟩. ⟨hal-02890692⟩
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ref_biblio: Christel Gervais, Christian Bonhomme, Danielle Laurencin. Recent directions in the solid-state NMR study of synthetic and natural calcium phosphates. Solid State Nuclear Magnetic Resonance, 2020, 107, pp.101663. ⟨10.1016/j.ssnmr.2020.101663⟩. ⟨hal-02570411⟩
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ref_biblio: Laëtitia Mayen, Nicholai D Jensen, Maximilien Desbord, Danielle Laurencin, Christel Gervais, et al.. Advances in the synthesis and structure of α-canaphite: a multitool and multiscale study. CrystEngComm, 2020, 22 (18), pp.3130-3143. ⟨10.1039/d0ce00132e⟩. ⟨hal-02873559⟩
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ref_biblio: Chia-Hsin Chen, Emeline Gaillard, Frédéric Mentink-Vigier, Kuizhi Chen, Zhehong Gan, et al.. Direct 17O-isotopic labeling of oxides using mechanochemistry. Inorganic Chemistry, 2020, 59 (18), pp.13050-13066. ⟨10.1021/acs.inorgchem.0c00208⟩. ⟨hal-02504692v2⟩
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ref_biblio: Laëtitia Mayen, Nicholai D Jensen, Danielle Laurencin, Olivier Marsan, Christian Bonhomme, et al.. A soft-chemistry approach to the synthesis of amorphous calcium ortho/pyrophosphate biomaterials of tunable composition. Acta Biomaterialia, 2020, 103, pp.333-345. ⟨10.1016/j.actbio.2019.12.027⟩. ⟨hal-02447805⟩
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ref_biblio: Guillaume Laurent, Pierre-Aymeric Gilles, William Woelffel, Virgile Barret-Vivin, Emmanuelle Gouillart, et al.. Denoising applied to spectroscopies-part II: Decreasing computation time. Applied Spectroscopy Reviews, 2020, 55 (3), pp.173-196. ⟨10.1080/05704928.2018.1559851⟩. ⟨hal-02063604⟩
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ref_biblio: Karol Rakotozandriny, Samantha Bourg, Paszkál Papp, Ágota Tóth, Dezső Horváth, et al.. Investigating CaOx Crystal Formation in Absence and Presence of Polyphenols under Microfluidic Conditions in Relation with Nephrolithiasis. Crystal Growth & Design, 2020, 20, pp.7683-7693. ⟨10.1021/acs.cgd.0c00929⟩. ⟨hal-02979866⟩
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ref_biblio: Guillaume Laurent, William Woelffel, Virgile Barret-Vivin, Emmanuelle Gouillart, Christian Bonhomme. Denoising applied to spectroscopies-part I: concept and limits. Applied Spectroscopy Reviews, 2019, 54 (7), pp.602-630. ⟨10.1080/05704928.2018.1523183⟩. ⟨hal-01879736⟩
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ref_biblio: Diana G. Ramírez-Wong, Christian Bonhomme, Sophie Demoustier-Champagne, Alain M. Jonas. Layer-by-layer assembly of brushes of vertically-standing enzymatic nanotubes. Journal of Colloid and Interface Science, 2018, 514, pp.592-598. ⟨10.1016/j.jcis.2017.12.063⟩. ⟨hal-02144948⟩
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ref_biblio: Christian Bonhomme, Xiaoling Wang, Ivan Hung, Zhehong Gan, Christel Gervais, et al.. Pushing the limits of sensitivity and resolution for natural abundance 43Ca NMR using ultra-high magnetic field (35.2 T). Chemical Communications, 2018, 54 (69), pp.9591-9594. ⟨10.1039/c8cc05193c⟩. ⟨hal-01861127⟩
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ref_biblio: Ivan Petit, Gustavo D. Belletti, Théau Debroise, Manuel J. Llansola-Portoles, Ivan T. Lucas, et al.. Vibrational Signatures of Calcium Oxalate Polyhydrates. ChemistrySelect, 2018, 3 (31), pp.8801-8812. ⟨10.1002/slct.201801611⟩. ⟨hal-02144971⟩
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ref_biblio: César Leroy, Fabien Aussenac, Laure Bonhomme-Coury, Akiyoshi Osaka, Satoshi Hayakawa, et al.. Hydroxyapatites: Key Structural Questions and Answers from Dynamic Nuclear Polarization. Analytical Chemistry, 2017, 89 (19), pp.10201 - 10207. ⟨10.1021/acs.analchem.7b01332⟩. ⟨hal-01611666⟩
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ref_biblio: Christel Gervais, Cameron Jones, Christian Bonhomme, Danielle Laurencin. Insight into the local environment of magnesium and calcium in low-coordination-number organo-complexes using 25 Mg and 43 Ca solid-state NMR: a DFT study. Acta Crystallographica Section C : Structural Chemistry [2014-..], 2017, 73 (3), pp.208 - 218. ⟨10.1107/S205322961601929X⟩. ⟨hal-01480332⟩
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ref_biblio: Daniel Lee, César Leroy, Charlene Crevant, Laure Bonhomme-Coury, Florence Babonneau, et al.. Interfacial Ca²⁺ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced ⁴³Ca NMR spectroscopy. Nature Communications, 2017, 8, pp.14104. ⟨10.1038/ncomms14104⟩. ⟨hal-01448516⟩
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ref_biblio: Kemie Ley-Ngardigal, Christèle Combes, Sébastien Teychené, Christian Bonhomme, Cristina Coelho-Diogo, et al.. Influence of Ionic Additives on Triclinic Calcium Pyrophosphate Dihydrate Precipitation. Crystal Growth & Design, 2017, 17 (1), pp.37-50. ⟨10.1021/acs.cgd.6b01128⟩. ⟨hal-01518197⟩
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ref_biblio: Thomas-Xavier Métro, Christel Gervais, Anthony Martinez, Christian Bonhomme, Danielle Laurencin. Unleashing the Potential of ¹⁷ O NMR Spectroscopy Using Mechanochemistry. Angewandte Chemie International Edition, 2017, 56 (24), pp.6803-6807 ⟨10.1002/anie.201702251⟩. ⟨hal-01527336⟩
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ref_biblio: Danielle Laurencin, François Ribot, Christel Gervais, Adrian J. Wright, Annabelle Baker, et al.. 87Sr, 119Sn, 127I Single and {1H/19F}-Double Resonance Solid-State NMR Experiments: Application to Inorganic Materials and Nanobuilding Blocks. ChemistrySelect, 2016, 1 (15), pp.4509-4519. ⟨10.1002/slct.201600805⟩. ⟨hal-01378175⟩
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ref_biblio: J.A. Lehmann-Horn, J.-F Jacquinot, J.-C. Ginefri, Christian Bonhomme, D Sakellariou. Monolithic MACS micro resonators. Journal of Magnetic Resonance, 2016, 271, pp.46-51. ⟨10.1016/j.jmr.2016.07.013⟩. ⟨cea-01355275⟩
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ref_biblio: Gauthier J.-P. Deblonde, Cristina Coelho-Diogo, Alexandre Chagnes, Gérard Cote, Mark E. Smith, et al.. Multinuclear Solid-State NMR Investigation of Hexaniobate and Hexatantalate Compounds. Inorganic Chemistry, 2016, 55 (12), pp.5946 - 5956. ⟨10.1021/acs.inorgchem.6b00345⟩. ⟨hal-01429965⟩
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ref_biblio: Saad Sene, Marie Pizzoccaro, Joris Vezzani, Marc Reinholdt, Philippe Gaveau, et al.. Coordination Networks Based on Boronate and Benzoxaborolate Ligands. Crystals, 2016, Crystals, 6 (5), pp.48. ⟨10.3390/cryst6050048⟩. ⟨hal-01313402⟩
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ref_biblio: Pierre Gras, Annabelle Baker, Christèle Combes, Christian Rey, Stéphanie Sarda, et al.. From crystalline to amorphous calcium pyrophosphates: a solid state Nuclear Magnetic Resonance perspective. Acta Biomaterialia, 2016, 31, pp.348-357. ⟨10.1016/j.actbio.2015.10.016⟩. ⟨hal-01221038⟩
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ref_biblio: Dominique Bazin, David Portehault, Frederik Tielens, Jacques Livage, Christian Bonhomme, et al.. Urolithiasis: What can we learn from a Nature which dysfunctions?. Comptes Rendus. Chimie, 2016, 19 (11-12), pp.1558-1564. ⟨10.1016/j.crci.2016.01.019⟩. ⟨hal-01305461⟩
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ref_biblio: Dominique Bazin, César Leroy, Frederik Tielens, Christian Bonhomme, Laure Bonhomme-Coury, et al.. Hyperoxaluria is related to whewellite and hypercalciuria to weddellite: What happens when crystalline conversion occurs?. Comptes Rendus. Chimie, 2016, 19 (11-12), pp.1573-1579. ⟨10.1016/j.crci.2015.12.011⟩. ⟨hal-01297865⟩
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ref_biblio: Arnaud Dessombz, Gérard Coulibaly, Brahima Kirakoya, Richard W. Ouedraogo, Adama Lengani, et al.. Structural elucidation of silica present in kidney stones coming from Burkina Faso. Comptes Rendus. Chimie, 2016, 19 (11-12), pp.1573 - 1579. ⟨10.1016/j.crci.2016.06.012⟩. ⟨hal-01427891⟩
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ref_biblio: G. Laffite, César Leroy, Christian Bonhomme, L. Bonhomme-Coury, Emmanuel Letavernier, et al.. Calcium oxalate precipitation by diffusion using laminar microfluidics: toward a biomimetic model of pathological microcalcifications. Lab on a Chip, 2016, 16 (7), pp.1157-1160. ⟨10.1039/C6LC00197A⟩. ⟨hal-01288757⟩
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ref_biblio: Diana Guadalupe Ramirez Wong, Cristina Coelho-Diogo, Carole Aimé, Christian Bonhomme, Alain M. Jonas, et al.. Effects of geometrical confinement in membrane pores on enzyme-based layer-by-layer assemblies. Applied Surface Science, 2015, 338, pp.154-162. ⟨10.1016/j.apsusc.2015.02.123⟩. ⟨hal-01274324⟩
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ref_biblio: Saad Sene, Sylvie Bégu, Christel Gervais, Guillaume Renaudin, Adel Mesbah, et al.. Intercalation of benzoxaborolate anions in layered double hydroxides: toward hybrid formulations for benzoxaborole drugs. Chemistry of Materials, 2015, 27 (4), pp.1242-1254. ⟨10.1021/cm504181w⟩. ⟨hal-01109256⟩
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ref_biblio: Dorothée Berthomieu, Christel Gervais, Guillaume Renaudin, Marc Reinholdt, Saad Sene, et al.. Coordination polymers based on alkylboronate ligands: synthesis, characterization, and computational modelling. European Journal of Inorganic Chemistry, 2015, pp.1182-1191. ⟨10.1002/ejic.201402561⟩. ⟨hal-01175713⟩
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ref_biblio: Marie-Alexandra Neouze, Martin Kronstein, Marco Litschauer, Michael Puchberger, Cristina Coelho, et al.. Exploring the Molecular Structure of Imidazolium-Silica-Based Nanoparticle Networks by Combining Solid-State NMR Spectroscopy and First-Principles Calculations. Chemistry - A European Journal, 2014, 20 (46), pp.15188-15196. ⟨10.1002/chem.201403730⟩. ⟨hal-01275058⟩
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ref_biblio: Frédérique Pourpoint, Julien Trébosc, Christian Bonhomme, Olivier Durupthy, Nathalie Steunou, et al.. Quantitative Analysis of the Proximities of OH Ligands and Vanadium Sites in a Polyoxovanadate Cluster Using Frequency-Selective H-1-V-51 Solid-State NMR Spectroscopy. Journal of Physical Chemistry C, 2014, 118 (32), pp.18580-18588. ⟨10.1021/jp505194q⟩. ⟨hal-01275061⟩
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ref_biblio: Pascal Man, Christian Bonhomme, Florence Babonneau. Denoising NMR time-domain signal by singular-value decomposition accelerated by graphics processing units. Solid State Nuclear Magnetic Resonance, 2014, 61-62, pp.28-34. ⟨10.1016/j.ssnmr.2014.05.001⟩. ⟨hal-01275072⟩
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ref_biblio: Christian Bonhomme, Christel Gervais, Danielle Laurencin. Recent NMR developments applied to organic-inorganic materials. Progress in Nuclear Magnetic Resonance Spectroscopy, 2014, 77, pp.1-48. ⟨10.1016/j.pnmrs.2013.10.001⟩. ⟨hal-00881233⟩
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ref_biblio: Olivier Fontaine, Amina Touidjine, Manuel Maréchal, Christian Bonhomme, François Ribot, et al.. One−pot Route To Class II Hybrid Ionogels Electrolytes. New Journal of Chemistry, 2014, 38 (5), pp.2008-2015. ⟨10.1039/C3NJ01272G⟩. ⟨hal-00922351⟩
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ref_biblio: Danielle Laurencin, Christian Bonhomme. RMN large bande des noyaux quadripolaires en phase solide : exemple de strontium-87. Techniques de l'Ingénieur, 2014, pp.IN-166. ⟨hal-01053752⟩
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ref_biblio: Elsa Alvarez, Alfonso Garcia-Marquez, Thomas Devic, Nathalie Steunou, Christian Serre, et al.. A biocompatible calcium bisphosphonate coordination polymer: towards a metal-linker synergistic therapeutic effect?. CrystEngComm, 2013, 15, pp.9899. ⟨10.1039/c3ce41346b⟩. ⟨hal-00881213⟩
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ref_biblio: Hélène Colas, Laure Bonhomme-Coury, Cristina Coelho Diogo, Frederik Tielens, Florence Babonneau, et al.. Whewellite, CaC2O4*H2O: structural study by a combined NMR, crystallography and modelling approach. CrystEngComm, 2013, 15, pp.8840. ⟨10.1039/c3ce41201f⟩. ⟨hal-00881226⟩
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ref_biblio: Saad Sene, B. Bouchevreau, Charlotte Martineau, Christel Gervais, Christian Bonhomme, et al.. Structural study of calcium phosphonates: a combined synchrotron powder diffraction, solid-state NMR and first-principle calculations approach. CrystEngComm, 2013, 15, pp.8763. ⟨10.1039/c3ce40981c⟩. ⟨hal-00881221⟩
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ref_biblio: Stuart Miller, Elsa Alvarez, Lucie Fradcourt, Thomas Devic, Stefan Wuttke, et al.. A rare example of a porous Ca-MOF for the controlled release of biologically active NO. Chemical Communications, 2013, 49, pp.7773. ⟨10.1039/C3CC41987H⟩. ⟨hal-00823982⟩
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ref_biblio: Satoshi Hayakawa, Tomoko Kanaya, Kanji Tsuru, Yuki Shirosaki, Akiyoshi Osaka, et al.. Heterogeneous structure and in vitro degradation behavior of wet-chemically derived nanocrystalline silicon-containing hydroxyapatite particles. Acta Biomaterialia, 2013, 9 (1), pp.4856-4867. ⟨10.1016/j.actbio.2012.08.024⟩. ⟨hal-01468405⟩
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ref_biblio: Saad Sene, Marc Reinholdt, Guillaume Renaudin, Dorothée Berthomieu, Claudio Zicovich-Wilson, et al.. Boronate Ligands in Materials: Determining Their Local Environment by Using a Combination of IR/Solid-State NMR Spectroscopies and DFT Calculations. Chemistry - A European Journal, 2013, 19, pp.880-891. ⟨10.1002/chem.201203560⟩. ⟨hal-00784863⟩
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ref_biblio: Hélène Colas, Laure Bonhomme-Coury, Cristina Coelho Diogo, Frederik Tielens, Florence Babonneau, et al.. Whewellite, CaC2O4⋅H2O: structural study by a combined NMR, crystallography and modelling approach. CrystEngComm, 2013, 15 (43), pp.8840. ⟨10.1039/c3ce41201f⟩. ⟨hal-04152780⟩
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ref_biblio: Christian Bonhomme, Christel Gervais, Florence Babonneau, Cristina Coelho, Frédérique Pourpoint, et al.. First-Principles Calculation of NMR Parameters Using the Gauge Including Projector Augmented Wave Method: A Chemist’s Point of View. Chemical Reviews, 2012, 112 (11), pp.5733 - 5779. ⟨10.1021/cr300108a⟩. ⟨hal-01468419⟩
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ref_biblio: Vlad Badilita, Birgit Fassbender, Kai Kratt, Alan Wong, Christian Bonhomme, et al.. Microfabricated Inserts for Magic Angle Coil Spinning (MACS) Wireless NMR Spectroscopy. PLoS ONE, 2012, 7 (8), pp.e42848. ⟨10.1371/journal.pone.0042848⟩. ⟨hal-01468505⟩
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ref_biblio: Christian Bonhomme, Christel Gervais, Nicolas Folliet, Frédérique Pourpoint, Cristina Coelho Diogo, et al.. (87)Sr solid-state NMR as a structurally sensitive tool for the investigation of materials: antiosteoporotic pharmaceuticals and bioactive glasses.. Journal of the American Chemical Society, 2012, 134 (30), pp.12611-12628. ⟨10.1021/ja303505g⟩. ⟨hal-00726394⟩
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ref_biblio: Florence Babonneau, Christian Bonhomme, Christel Gervais, Thierry Azaïs, Guillaume Laurent, et al.. Les spins nucléaires : des espions pour explorer la structure des matériaux. L'Actualité Chimique, 2012, Danses avec les spins: la RMN en chimie, 364-365, pp.73-81. ⟨hal-01520904⟩
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ref_biblio: Ondrej Nikel, Danielle Laurencin, Christian Bonhomme, Grazyna E. Sroga, Silke Besdo, et al.. Solid State NMR Investigation of Intact Human Bone Quality: Balancing Issues and Insight into the Structure at the Organic−Mineral Interface. Journal of Physical Chemistry C, 2012, 116, pp.6320-6331. ⟨10.1021/jp2125312⟩. ⟨hal-00687826⟩
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ref_biblio: S. Derenne, C. Coelho, C. Anquetil, Cyril Szopa, A. S. Rahman, et al.. New insights into the structure and chemistry of Titan's tholins via13C and 15N solid state nuclear magnetic resonance spectroscopy. Icarus, 2012, 221 (2), pp.844-853. ⟨10.1016/j.icarus.2012.03.003⟩. ⟨hal-00678245⟩
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ref_biblio: Nathalie Steunou, Christine Mousty, Olivier Durupthy, Cécile Roux, Guillaume Laurent, et al.. A general route to nanostructured M[V3O8] and M-x[V6O16] (x=1 and 2) and their first evaluation for building enzymatic biosensors. Journal of Materials Chemistry, 2012, 22 (30), pp.15291-15302. ⟨10.1039/c2jm30485f⟩. ⟨hal-01461422⟩
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ref_biblio: Nicolas Folliet, Claire Roiland, Sylvie Bégu, Anne Aubert, Tzonka Mineva, et al.. Investigation of the interface in silica-encapsulated liposomes by combining solid state NMR and first principles calculations.. Journal of the American Chemical Society, 2011, 133 (42), pp.16815-16827. ⟨10.1021/ja201002r⟩. ⟨hal-00692389⟩
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ref_biblio: A. Li, D. Wang, J. Xiang, Robert Newport, Marc Reinholdt, et al.. Insights into new calcium phosphosilicate xerogels using an advanced characterization methodology. Journal of Non-Crystalline Solids, 2011, 357, pp.3548-3555. ⟨10.1016/j.jnoncrysol.2011.07.003⟩. ⟨hal-00615212⟩
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ref_biblio: Marc Reinholdt, Jonas Croissant, Lidia Di Carlo, Dominique Granier, Philippe Gaveau, et al.. Synthesis and Characterization of Crystalline Structures Based on Phenylboronate Ligands Bound to Alkaline Earth Cations. Inorganic Chemistry, 2011, 50, pp.7802. ⟨10.1021/ic200961a⟩. ⟨hal-00615204⟩
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ref_biblio: Danielle Laurencin, Neyvis Almora-Barrios, Nora H. de Leeuw, Christel Gervais, Christian Bonhomme, et al.. Magnesium incorporation into hydroxyapatite. Biomaterials, 2011, 32 (7), pp.1826-1837. ⟨10.1016/j.biomaterials.2010.11.017⟩. ⟨hal-00556834⟩
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ref_biblio: Frédérique Pourpoint, Cristina Coelho, Christel Gervais, Christian Bonhomme, Franck Fayon, et al.. High-resolution solid state NMR experiments for the characterization of calcium phosphate biomaterials and biominerals. Journal of Materials Research, 2011, 26, pp.2355-2368. ⟨10.1557/jmr.2011.250⟩. ⟨hal-00638531⟩
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ref_biblio: F. Babonneau, Niki Baccile, G. Laurent, J. Maquet, T. Azais, et al.. Solid-state nuclear magnetic resonance: A valuable tool to explore organic-inorganic interfaces in silica-based hybrid materials.. Comptes Rendus. Chimie, 2010, 13 (1-2), pp.58-68. ⟨10.1016/j.crci.2009.08.001⟩. ⟨hal-00462099⟩
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ref_biblio: Christian Bonhomme, C. Gervais, C. Coelho, F. Pourpoint, T. Azaïs, et al.. New perspectives in the PAW/GIPAW (Gauge Including Projected Augmented Wave) approach: JP-O-Si coupling constants, antisymmetric parts of shift tensors and NQR predictions. Magnetic Resonance in Chemistry, 2010, 48, pp.S86-S102. ⟨10.1002/mrc.2635⟩. ⟨hal-00608506⟩
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ref_biblio: S. Gomes, G. Renaudin, Adel Mesbah, Edouard Jallot, Christian Bonhomme, et al.. Thorough analysis of silicon substitution in biphasic calcium phosphate bioceramics: A multi-technique study. Acta Biomaterialia, 2010, 6 (8), pp.3264-3274. ⟨10.1016/j.actbio.2010.02.034⟩. ⟨hal-00492332⟩
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ref_biblio: L. Truflandier, Florent Boucher, Christophe Payen, R. Hajja, Y. Millot, et al.. DFT-NMR Investigation and V-51 3QMAS Experiments for Probing Surface OH Ligands and the Hydrogen-Bond Network in a Polyoxovanadate Cluster: The Case of Cs-4[H2V10O28]center dot 4H(2)O. Journal of the American Chemical Society, 2010, 132 (13), pp.4653. ⟨10.1021/ja908973y⟩. ⟨hal-00477290⟩
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ref_biblio: Céline Chizallet, H. Petitjean, G. Costentin, H. Lauron-Pernot, J. Maquet, et al.. Identification of the OH groups responsible for kinetic basicity on MgO surfaces by 1H MAS NMR. Journal of Catalysis, 2009, pp.175-179. ⟨10.1016/J.jcat.2009.09.003⟩. ⟨hal-00446808⟩
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ref_biblio: Danielle Laurencin, Christel Gervais, Alan Wong, Cristina Coelho, Francesco Mauri, et al.. Implementation of High Resolution 43Ca Solid State NMR Spectroscopy: Toward the Elucidation of Calcium Sites in Biological Materials. Journal of the American Chemical Society, 2009, 131, pp.13430. ⟨10.1021/ja904553q⟩. ⟨hal-00437583⟩
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ref_biblio: F. Mammeri, Christian Bonhomme, F. Ribot, F. Babonneau, S. Dirè. New Monofunctional POSS and Its Utilization as Dewetting Additive in Methacrylate Based Free-Standing Films.. Chemistry of Materials, 2009, 21, pp.4163-4171. ⟨10.1021/cm900339h⟩. ⟨hal-00421891⟩
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ref_biblio: C. Gervais, L. Bonhomme-Coury, Francesco Mauri, F. Babonneau, Christian Bonhomme. GIPAW (gauge including projected augmented wave) and local dynamics in 13C and 29Si solid state NMR: the study case of silsesquioxanes (RSIO1.5)8. Physical Chemistry Chemical Physics, 2009, 11, pp.6953-6961. ⟨10.1039/b907450c⟩. ⟨hal-00411209⟩
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ref_biblio: Guilhem Arrachart, Gaëlle Creff, Hubert Wadepohl, Christophe Blanc, Christian Bonhomme, et al.. Nanostructuring of Hybrid Silicas through a Self-Recognition Process. Chemistry - A European Journal, 2009, 15 (20), pp.5002. ⟨10.1002/chem.200802748⟩. ⟨hal-01224956⟩
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ref_biblio: S. de Monredon-Senani, Christian Bonhomme, F. Ribot, F. Babonneau. Covalent grafting of organoalkoxysilanes on silica surfaces in water-rich medium as evidenced by 29 Si NMR. Journal of Sol-Gel Science and Technology, 2009, 50, pp.152-157. ⟨10.1007/S10971-009-1920-7⟩. ⟨hal-00411126⟩
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ref_biblio: Christel Gervais, Danielle Laurencin, Alan Wong, Frédérique Pourpoint, John Labram, et al.. New perspectives on calcium environments in inorganic materials containing calcium-oxygen bonds: A combined computational-experimental 43Ca NMR approach.. Chemical Physics Letters, 2008, 464, pp.42-48. ⟨10.1016/j.cplett.2008.09.004⟩. ⟨hal-00358177⟩
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ref_biblio: Guilhem Arrachart, Carole Carcel, Joël J E Moreau, Geoffrey Hartmeyer, Bruno Alonso, et al.. Organo-silicas based on purine-pyrimidine base pairs assemblies : a solid state NMR point of view. Journal of Materials Chemistry, 2008, 18, pp.392-399. ⟨10.1039/b714785f⟩. ⟨hal-00189966⟩
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ref_biblio: C. Coelho, T. Azais, Christian Bonhomme, L. Bonhomme-Coury, C. Boissière, et al.. Efficiency of dipolar and J-derived solid-state NMR techniques for a new pair of nuclei {31P,29Si}. Towards the characterization of Si-O-P mesoporous materials. Comptes Rendus. Chimie, 2008, 11, pp.387-397. ⟨10.1016/j.crci.2007.09.012⟩. ⟨hal-00267398⟩
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ref_biblio: O. Durupthy, J. Maquet, Christian Bonhomme, T. Coradin, J. Livage, et al.. Room temperature sol-gel synthesis of crystalline [V3O8]. Probing the hydration level of the interlamellar space by 51V and 133Cs MAS NMR spectroscopy.. Journal of Materials Chemistry, 2008, 18, pp.3702-3712. ⟨hal-00348253⟩
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ref_biblio: Olivier Durupthy, Jocelyne Maquet, Christian Bonhomme, Thibaud Coradin, Jacques Livage, et al.. Room temperature sol–gel synthesis of crystalline Cs[V3O8]. Probing the hydration level of the interlamellar space by 51V and 133Cs MAS NMR spectroscopy. Journal of Materials Chemistry, 2008, 18 (31), pp.3702. ⟨10.1039/b804397c⟩. ⟨hal-02354059⟩
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ref_biblio: G. Gasquerès, Christian Bonhomme, J. Maquet, F. Babonneau, S. Hayakawa, et al.. Revisiting silicate substituted hydroxyapatite by solid state NMR.. Magnetic Resonance in Chemistry, 2008, 46, pp.342-346. ⟨hal-00347554⟩
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ref_biblio: S. Hayakawa, A. Osaka, K. Tsuru, E. Fujii, K. Kawabata, et al.. Synthesis and characterization of Mg-containing nano-apatite.. Key Engineering Materials, 2008, 361, pp.47-50. ⟨hal-00347519⟩
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ref_biblio: T. Kanaya, K. Tsuru, S. Hayakawa, A. Osaka, E. Fujii, et al.. Structure and in vitro solubility of silicon-substituted hydroxyapatite.. Key Engineering Materials, 2008, 361, pp.63-66. ⟨hal-00347525⟩
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ref_biblio: Frédérique Pourpoint, Christelle Gervais, Laure Bonhomme-Coury, Francesco Mauri, Bruno Alonso, et al.. Calcium phosphates : First-principles calculations vs. solid-state NMR experiments.. Comptes Rendus. Chimie, 2008, 11, pp.398-406. ⟨hal-00347950⟩
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ref_biblio: Céline Chizallet, Guylène Costentin, Helene Lauron-Pernot, Michel Che, Christian Bonhomme, et al.. Study of the Structure of OH Groups on MgO by 1D and 2D 1 H MAS NMR Combined with DFT Cluster Calculations. Journal of Physical Chemistry C, 2007, 111 (49), pp.18279 - 18287. ⟨10.1021/jp077089g⟩. ⟨hal-01896667⟩
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ref_biblio: Gilles Guerrero, Christel Gervais, Christian Bonhomme, Cristina Coelho, Thierry Azaïs, et al.. First principles NMR calculations of phenylphosphinic acid C6H5HPO(OH): Assignments, orientation of tensors by local field experiments and effect of molecular motion. Journal of Magnetic Resonance, 2007, 187 (1), pp.131-140. ⟨10.1016/j.jmr.2007.03.018⟩. ⟨hal-00186742⟩
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ref_biblio: Niki Baccile, Guillaume Laurent, Christian Bonhomme, Plinio Innocenzi, Florence Babonneau. Solid-State NMR Characterization of the Surfactant−Silica Interface in Templated Silicas: Acidic versus Basic Conditions. Chemistry of Materials, 2007, 19 (6), pp.1343-1354. ⟨10.1021/cm062545j⟩. ⟨hal-01455158⟩
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ref_biblio: C. Coelho, T. Azais, L. Bonhomme-Coury, G. Laurent, Christian Bonhomme. Efficiency of the refocused 31P-29Si MAS-J-INEPT NMR experiment for the characterization of silicophosphate crystalline phases and amorphous gels.. Inorganic Chemistry, 2007, 46 (4), pp.1379-1387. ⟨10.1021/ic061964f⟩. ⟨hal-00326965⟩
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ref_biblio: Bruno Alonso, Guilhem Arrachart, Florence Babonneau, Christian Bonhomme, Wong Chi Man Michel, et al.. Interfaces involving biomolecules and inorganic materials : a solid state NMR approach. Materials Research Society Symposia Proceedings, 2007, 1008, pp.T02-09. ⟨10.1557/PROC-1008-T02-09⟩. ⟨hal-00222778⟩
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ref_biblio: Marion Bardy, Christian Bonhomme, Emmanuel Fritsch, Jocelyne Maquet, Redouane Hajjar, et al.. Al speciation in tropical podzols of the upper Amazon Basin: A solid-state 27Al MAS and MQMAS NMR study. Geochimica et Cosmochimica Acta, 2007, 71 (13), pp.3211-3222. ⟨10.1016/j.gca.2007.04.024⟩. ⟨hal-00279729⟩
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ref_biblio: Marion Bardy, Christian Bonhomme, E. Fritsch, J. Maquet, R. Hajjar, et al.. Al speciation in tropical podzols of the upper Amazon Basin: A solid-state 27Al MAS and MQMAS NMR study. Geochimica et Cosmochimica Acta, 2007, 71, pp.3211-3222. ⟨10.1016/j.gca.2007.04.024⟩. ⟨bioemco-00177895⟩
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ref_biblio: Christian Bonhomme, Cristina Coelho, Niki Baccile, Christel Gervais, Thierry Azais, et al.. Advanced solid state NMR techniques for the characterisation of sol-gel derived materials.. Accounts in Chemical Research, 2007, 40, pp.738-746. ⟨hal-00334266⟩
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ref_biblio: Satoshi Hayakawa, Kanae Ando, Kanji Tsuru, Akiyoshi Osaka, Eiji Fujii, et al.. Structural characterization and protein adsorption property of hydroxyapatite particles modified with zinc ions.. Journal of the American Ceramic Society, 2007, 90, pp.565-569. ⟨hal-00334156⟩
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ref_biblio: Frédérique Pourpoint, Christel Gervais, Laure Bonhomme-Coury, Thierry Azais, Cristina Coelho, et al.. Calcium Phosphates and Hydroxyapatite: Solid State NMR Experiments and First Principles Calculations. Applied Magnetic Resonance, 2007, 32, pp.435-457. ⟨10.1007/s00723-007-0040-1⟩. ⟨hal-00343640⟩
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ref_biblio: Michel Wong Chi Man, Guilhem Arrachart, Carole Carcel, Joël J E Moreau, Christian Bonhomme, et al.. Nanostructuring of hybrid silicas : new approach to bridges silsesquioxanes with purine-pyrimidine base pairs as bridging units. Materials Research Society Symposia Proceedings, 2007, 1007, pp.S02-03. ⟨10.1557/PROC-1007-S02-03⟩. ⟨hal-00222769⟩
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ref_biblio: C. Coelho, F. Babonneau, T. Azais, L. Bonhomme-Coury, J. Maquet, et al.. Chemical bonding in silicophosphate gels : Contribution of dipolar and J-derived solid state NMR techniques. Journal of Sol-Gel Science and Technology, 2006, 40 (2-3), pp.181-189. ⟨10.1007/s10971-006-7431-x⟩. ⟨hal-00107473⟩
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ref_biblio: Christian Bonhomme, C. Coelho, T. Azais, L. Bonhomme-Coury, F. Babonneau, et al.. Some triple resonance experiments in solid-state CP MAS NMR : 51V/29Si, 31P/13C and 29Si/13C. Comptes Rendus. Chimie, 2006, 9, pp.466-471. ⟨hal-00107475⟩
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ref_biblio: C. Coelho, T. Azais, L. Bonhomme-Coury, J. Maquet, Dominique Massiot, et al.. Application of the MAS-J-HMQC experiment to a new pair of nuclei {29Si,31P}: Si5O(PO4)6 and SiP2O7 polymorphs. Journal of Magnetic Resonance, 2006, 179, pp.106-111. ⟨10.1016/j.jmr.2005.11.015⟩. ⟨hal-00016038⟩
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ref_biblio: Eiji Fujii, Mizuki Ohkubo, Kanji Tsuru, Satoshi Hayakawa, Akiyoshi Osaka, et al.. Selective protein adsorption property and characterization of nano-crystalline zinc-containing hydroxyapatite. Acta Biomaterialia, 2006, 2, pp.69-74. ⟨hal-00077562⟩
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ref_biblio: S. Hayakawa, K. Ohnishi, K. Tsuru, A. Osaka, E. Fujii, et al.. Selective protein adsorption property and structure of nano-crystalline hydroxy-carbonate apatite. Key Engineering Materials, 2006, 309-311, pp.503-506. ⟨hal-00107476⟩
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ref_biblio: Christian Bonhomme, Florence Babonneau, Lydie Camus. Silica and hybrid silica gels revisited : new insight by solid state nuclear magnetic resonance. Materials Research Society Symposia Proceedings, 2005, 847, pp.EE4.6.1. ⟨hal-00077212⟩
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ref_biblio: Olivier Durupthy, Nathalie Steunou, T. Coradin, Jocelyne Maquet, Christian Bonhomme, et al.. Influence of pH and ionic strength on vanadium (v) oxides formation. From V2O5.nH2O gels to crystalline NaV3O8.1.5H2O. Journal of Materials Chemistry, 2005, 15, pp.1090-1098. ⟨hal-00022434⟩
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ref_biblio: Christel Gervais, Ray Dupree, Kevin J. Pike, Christian Bonhomme, Mickael Profeta, et al.. Combined First-Principles Computational and Experimental Multinuclear Solid-State NMR Investigation of Amino Acids.. Journal of Physical Chemistry A, 2005, 109, pp.6960-6969. ⟨10.1021/jp0513925⟩. ⟨hal-00020231⟩
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ref_biblio: Maggy Hologne, Philippe Bertani, Thierry Azais, Christian Bonhomme, Jerôme Hirschinger. 1H/31P distance determination by solid state NMR in multiple-spin systems. Solid State Nuclear Magnetic Resonance, 2005, 28, pp.50-56. ⟨hal-00071030⟩
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ref_biblio: Clarisse Lejeune, Cristina Coelho, Laure Bonhomme-Coury, Thierry Azais, Jocelyne Maquet, et al.. Studies of silicophosphate derivatives by 31P 29Si CP MAS NMR. Solid State Nuclear Magnetic Resonance, 2005, 27, pp.242-246. ⟨hal-00071045⟩
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ref_biblio: Christel Gervais, Mickaël Profeta, Vincent Lafond, Christian Bonhomme, Thierry Azaïs, et al.. Combined ab initio computational and experimental multinuclear solid-state magnetic resonance study of phenylphosphonic acid.. Magnetic Resonance in Chemistry, 2004, 42, pp.445-452. ⟨10.1002/mrc.1360⟩. ⟨hal-00086010⟩
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ref_biblio: C. Bonhomme, T. Azaïs, L. Bonhomme, J. Livage, J-B. d'Espinose, et al.. High-Resolution Solid-State Nmr: a Versatile Tool for the Study of AI-O-P Clusters. Phosphorus, Sulfur, and Silicon and the Related Elements, 2001, 168 (1), pp.243-248. ⟨10.1080/10426500108546561⟩. ⟨hal-02049292⟩
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ref_biblio: Christel Gervais, Florence Babonneau, Jocelyne Maquet, Christian Bonhomme, Dominique Massiot, et al.. 15N Cross-Polarization using the Inversion-Recovery Cross-Polarization Technique and 11B Magic Angle Spinning NMR Studies of Reference Compounds Containing B-N Bonds. Magnetic Resonance in Chemistry, 1998, 36 (6), pp.407-414. ⟨10.1002/(SICI)1097-458X(199806)36:6%3C407::AID-OMR295%3E3.0.CO;2-Y⟩. ⟨hal-04947624⟩
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ref_biblio: Christian Bonhomme, Florence Babonneau, Jocelyne Maquet, Jacques Livage, Michel Vaultier, et al.. Studies of model organic and inorganic compounds by 15N CP MAS NMR using Inversion Recovery Cross Polarization. Journal de Chimie Physique, 1995, 92, pp.1881-1884. ⟨hal-04947661⟩
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ref_biblio: C. Semidor-Signoret, P. Jouenne, Christian Bonhomme, Pascal Joanne. QUALITÉ ACOUSTIQUE DE QUELQUES SALLES DE CONCERT EN ALLEMAGNE. Journal de Physique IV Proceedings, 1992, Deuxième Congrès Français d'Acoustique / Second French Conference on Acoustics, 02 (C1), pp.C1-147-C1-150. ⟨10.1051/jp4:1992128⟩. ⟨jpa-00251199⟩
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ref_biblio: M. Buenerd, Christian Bonhomme, D. Lebrun, P. Martin, J. Chauvin, et al.. Inelastic scattering of 108.5 MeV $^3$He particles at very small momentum transfer to the giant monopole resonance of $^{90}$Zr and $^{208}$Pb. Physics Letters B, 1979, 84, pp.305-308. ⟨10.1016/0370-2693(79)90045-5⟩. ⟨in2p3-00008845⟩
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Conference papers

ref_biblio: Guillaume P. Laurent, Christian Bonhomme. Can we improve solid-state NMR sensitivity without DNP ?. GERM 2023 – Résonance Magnétique aux Extrêmes, https://germ2023.sciencesconf.org/, Jun 2023, Murol, France. ⟨hal-04459500⟩
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ref_biblio: Guillaume Laurent, Christian Bonhomme. Simulating and denoising NMR spectra under Python. 5èmes Journées nationales du DEVeloppement (JDEV2020), Jul 2020, Rennes, France. ⟨hal-03013180⟩
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ref_biblio: Guillaume Laurent, Winh-Chhunn Teh, Jochen A. Lehmann-Horn, Dimitrios Sakellariou, Christian Bonhomme. Microcoils to improve solid-state NMR sensitivity. XXXI ème Congrès du GERM, Approches rapides en RMN, May 2019, Saint-Pierre d’Oléron, France. ⟨hal-02156281⟩
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ref_biblio: Christian Bonhomme, P.-L Giscard. A New Approach of Ordered Exponential in NMR: the Path-Sum. 60th Experimental Nuclear Magnetic Resonance Conference, Apr 2019, Pacific Grove, CA, United States. ⟨hal-02097616⟩
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ref_biblio: Guillaume Laurent, Christian Bonhomme. Non-uniform sampling applied to solid-state NMR. RMN structurale dans le Bassin Parisien, Mar 2018, Orléans, France. ⟨hal-01745319⟩
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ref_biblio: Morgane Pellerin, Cristina Coelho-Diogo, Christian Bonhomme, Nadia Touatib, Laurent Binet, et al.. Optical properties and mechanisms in Cr³⁺ , Bi³⁺-codoped oxide-based spinel nanoparticles. SPIE OPTO, 2017, San Francisco, CA, United States. pp.101000B, 1-7, ⟨10.1117/12.2253852⟩. ⟨hal-02175634⟩
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ref_biblio: Christian Bonhomme, Cristina Coelho-Diogo, César Leroy, Dominique Bazin, Florence Babonneau, et al.. Solid State NMR: a Pertinent Tool of Investigation for Calcium Derivatives. The Study Case of Randall’s Plaque.. 50th Annual Scientific Meeting of the European Society for Clinical Investigation Paris, Apr 2016, Paris, France. pp.8.03. ⟨hal-01329379⟩
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ref_biblio: Guillaume Laurent, William Woelffel, Virgile Barret-Vivin, Emmanuelle Gouillart, Christian Bonhomme. Spectra denoising: using graphic cards ?. RMN structurale dans le Bassin Parisien, Jan 2016, Thiais, France. ⟨hal-01277415⟩
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ref_biblio: Guillaume Laurent, William Woelffel, Virgile Barret-Vivin, Emmanuelle Gouillart, Christian Bonhomme. Performance du SVD pour débruiter les spectres RMN et Raman. c2i-2016 : 7ème Colloque Interdisciplinaire en Instrumentation, Jan 2016, Saint-Nazaire, France. pp.1-8. ⟨hal-01277387⟩
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ref_biblio: Kristell Quelever, Benoit Derat, T. Coradin, Olivier Meyer, Christian Bonhomme. Characterization of head and body phantoms for radiofrequency dosimetry, up to 6 GHz. RF and Wireless Technologies for Biomedical and Healthcare Applications (IMWS-BIO), Sep 2015, Taipei, Taiwan. pp.38-39, ⟨10.1109/IMWS-BIO.2015.7303764⟩. ⟨hal-01244460⟩
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ref_biblio: Guillaume Laurent, Christian Bonhomme, Dimitris Sakellariou. Microbobines et RMN en phase solide. Instrumenter et innover en chimie physique pour préparer l'avenir, Emmanuel Maisonhaute, Jan 2015, Paris, France. ⟨hal-01139041⟩
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ref_biblio: G. Deblonde, A. Chagnes, G. Cote, S. Belair, A. Moncomble, et al.. UV-vis and solid state MAS NMR as efficient techniques to investigate niobium and tantalum speciation in alkaline media. 6th International Conference of Hydrometallurgy, Aug 2014, Pékin, China. ⟨hal-01187175⟩
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ref_biblio: Kristell Quelever, Benoit Derat, Olivier Meyer, T. Coradin, Christian Bonhomme. A Dispersion Modeling Approach for Designing Broadband Tissue-Simulating Fluids. EMC'14, May 2014, Tokyo, Japan. ⟨hal-01100031⟩
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ref_biblio: Kristell Quelever, Olivier Meyer, Benoit Derat, T. Coradin, Christian Bonhomme. Conception et rationalisation d'un nouveau simulant de tissus biologiques pour la dosimétrie radiofréquence. JCMM 2014, IETR (UMR CNRS 6164) et ISCR (UMR CNRS 6226), Mar 2014, Nantes, France. pp.ID 40. ⟨hal-01095825⟩
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ref_biblio: Damien Di-Marco, Laura Molina Jotel, Fabrice Rossignol, Thierry Chartier, Christian Bonhomme, et al.. New catalysts for intensified H2 production by steam methane reforming. 13th International Conference on the European Ceramic Society, ECerS 2013, Jun 2013, Limoges, France. ⟨hal-00947044⟩
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ref_biblio: Kristell Quelever, Olivier Meyer, Benoit Derat, T. Coradin, Christian Bonhomme. Rational Chemical Design of Broadband Tissue-Simulating Liquids. BioEM2013, Jun 2013, Thessaloniki, Greece. 3 p. ⟨hal-00931070⟩
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ref_biblio: Y. Wang, N. Nassif, L. Bonhomme, Christian Bonhomme, F. Babonneau, et al.. Towards a Better Structural Characterization of Substituted Hydroxyapatites. 3rd International Congress on Ceramics ICC3, Nov 2010, Osaka, Japan. pp.S13-026. ⟨in2p3-00609272⟩
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ref_biblio: Danielle Laurencin, G. Guerrero, J. Amalric, Christian Bonhomme, C. Gervais, et al.. Advanced Solid State NMR Techniques for the Investigation of the Organic-Mineral Interfaces in Biomaterials.. MRS Fall Meeting, Nov 2009, Boston, United States. pp.1236-SS08-02, ⟨10.1557/PROC-1236-SS08-02⟩. ⟨hal-00492955⟩
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ref_biblio: Frédérique Pourpoint, Christel Gervais, Laure Bonhomme-Coury, Francesco Mauri, Bruno Alonso, et al.. Calcium phosphates: First-principles calculations vs. solid-state NMR experiments. GERM 2007, 2007, France. pp.398-406, ⟨10.1016/j.crci.2007.09.011⟩. ⟨hal-00277151⟩
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ref_biblio: Cristina Coelho, Nadia Benharbya, Cristel Gervais, Thierry Azaïs, Laure Bonhomme-Coury, et al.. Dipolar and J- Derived Solid State NMR Techniques and First Principles Calculations Applied to the Structure of Silicophosphates and to the Characterization of Phosphonate Grafting on Silica Nanoparticles. 2006 MRS Fall Meeting, Nov 2006, Boston, MA, United States. pp.0984-MM14-05, 1-6, ⟨10.1557/PROC-984-0984-MM14-05⟩. ⟨hal-02351173⟩
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ref_biblio: Christian Bonhomme, M. Wong Chi Man, B. Alonso, Guilhem Arrachart, G. Hartmeyer, et al.. RMN du solide : une approche des matériaux hybrides et des nanomatériaux. Matériaux 2006, Nov 2006, Dijon, France. CM-10-0312 (p150). ⟨hal-00394341⟩
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ref_biblio: Fayna Mammeri, Najiba Douja, Christian Bonhomme, François Ribot, Florence Babonneau, et al.. Modification and characterization of Si-based nanobuilding blocks precursors for hybrid materials. 2005, pp.EE13.26.1-EE13.26.6. ⟨hal-00018693⟩
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ref_biblio: Claude Rebattet, C. Bonhomme, Jean-Pierre Franc, Michel Riondet. Investigation of thermodynamic effect in cavitating inducers. An experimental study on French university facilities. 4th International Conference on Launcher Technology, Space launcher liquid propulsion, Dec 2003, Liege, Belgium. ⟨hal-00216176⟩
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ref_biblio: Claude Rebattet, Jean-Pierre Franc, Alain Coulon, C. Bonhomme. Investigation of thermodynamic effect in cavitating inducers. An experimental study on French university facilities. 1st European Hydrogen Energy Conference, Sep 2002, Grenoble, France. ⟨hal-00216174⟩
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ref_biblio: P. Martin, M. Buenerd, D. Lebrun, G. Perrin, P. de Saintignon, et al.. Systematic investigation of the giant monopole resonance with 108.5 MeV $^3$He through the periodic table. 1980 RCNP International Symposium on Highly Excited States in Nuclear Reactions, May 1980, Suita Osaka, Japan. pp.131-144. ⟨in2p3-00007451⟩
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Book sections

ref_biblio: Bruno Alonso, Christian Bonhomme, Christel Gervais, Flavien Guenneau, Danielle Laurencin, et al.. Nuclear Magnetic Resonance as a Tool for the Investigation of Interfaces and Textures in Nanostructured Hybrid Materials. Hybrid Organic-Inorganic Interfaces: Towards Advanced Functional Materials, 2017, ⟨10.1002/9783527807130.ch20⟩. ⟨hal-01936830⟩
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Patents

ref_biblio: Christian Bonhomme, Thierry Chartier, Fabrice Rossignol, R. Faure, P. del Gallo, et al.. DISPOSITIF D'EPURATION DES GAZ D'ECHAPPEMENT D'UN MOTEUR THERMIQUE COMPRENANT UN SUPPORT CERAMIQUE FRACTIONNE A L'ECHELLE NANOMETRIQUE. France, Patent n° : FR2991713. 2013, pp.27. ⟨hal-00942826⟩
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ref_biblio: P. del Gallo, Fabrice Rossignol, Thierry Chartier, R. Faure, Christian Bonhomme, et al.. Procédé d'assemblage de deux composants céramiques de même composition chimique élémentaire. France, N° de brevet: FR2976939. 2012, pp.30. ⟨hal-00942360⟩
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ref_biblio: P. del Gallo, Fabrice Rossignol, Thierry Chartier, R. Faure, Christian Bonhomme, et al.. Dispositif d'épuration des gaz d'échappement d'un moteur thermique comprenant un support céramique et une phase active ancrée mécaniquement dans le support. France, N° de brevet: FR2976823. 2012, pp.23. ⟨hal-00942377⟩
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ref_biblio: P. del Gallo, Fabrice Rossignol, Thierry Chartier, R. Faure, Christian Bonhomme, et al.. Dispositif d'épuration des gaz d'échappement d'un moteur thermique comprenant un support céramique et une phase active ancrée chimiquement et mécaniquement dans le support. France, N° de brevet: FR2976821. 2012, pp.25. ⟨hal-00942365⟩
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ref_biblio: K. Quelever, T. Coradin, Christian Bonhomme, Olivier Meyer, B. Derat. Composition simulating the dielectric properties of the human body. France, Patent n° : PCT/EP2012/074007. 2012. ⟨hal-00781278⟩
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Poster communications

ref_biblio: Guillaume Laurent, Christian Bonhomme. Improving solid-state NMR sensitivity using instrumentation, fast acquisition and post-processing. EUROpean MAgnetic Resonance meeting, EUROMAR, Jul 2018, Nantes, France. ⟨hal-01832993⟩
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ref_biblio: Guillaume Laurent, Christian Bonhomme. Non-uniform sampling & denoising applied to nuclear magnetic resonance. Spring School on Sparse Representations and Compressed Sensing, Apr 2016, Ilmenau, Germany. ⟨hal-01516795⟩
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ref_biblio: Guillaume Laurent, Pascal Ping Man, Christian Bonhomme. Spectra Denoising using Graphic Cards. XXVI e Conférence du GERM, “Simulation et Modélisation en RMN”, May 2015, Sète, France. . ⟨hal-01168997⟩
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ref_biblio: Claire Bourlieu-Lacanal, Sophie Chever, Olivia Ménard, Amélie Deglaire, F. Morgan, et al.. An insight into the interfacial composition and susceptibility to digestion of model infant formulas stabilized by milk polar lipids. The 11. Biennial ISSFAL Congress 2014, Jun 2014, Stockholm, Sweden. , 2014. ⟨hal-01209666⟩
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ref_biblio: Isabelle Luron, Karima Bouzerzour, Stéphanie Ferret-Bernard, Cindy Le Bourgot, Claire Bourlieu-Lacanal, et al.. Milk lipids in infant formulas modify the proteolysis, microbiota and intestinal physiology in neonatal piglets. The 11. Biennial ISSFAL Congress 2014, Jun 2014, Stockholm, Sweden. 2014. ⟨hal-01209667⟩
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ref_biblio: Isabelle Luron, Karima Bouzerzour, Stéphanie Ferret-Bernard, Cindy Le Bourgot, Claire Bourlieu-Lacanal, et al.. Addition of milk fat in infant formula impacts neonatal gut microbiota. The 11. Biennial ISSFAL Congress 2014, Jun 2014, Stockholm, Sweden. 2014. ⟨hal-01209668⟩
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ref_biblio: Cindy Le Bourgot, Karima Bouzerzour, Stéphanie Ferret-Bernard, Claire Bourlieu-Lacanal, Laurence Le Normand, et al.. Introduction of milk phospholipids and lipids in infant formula promotes the intestinal immune system maturation in neonatal piglets. 2 International Conference on Food Digestion, Mar 2013, Madrid, Spain. , 2013. ⟨hal-01209430⟩
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ref_biblio: Karima Bouzerzour, Stéphanie Ferret-Bernard, Olivia Ménard, F. Morgan, F. Cuinet, et al.. Impact of Casein / Whey proteins (Cns/WPs) ratio of infant formulas on in vivo protein digestion and gut physiology. 1 st international conference on Food Digestion, Mar 2012, Cesena, Italy. Cost Infogest, 2012. ⟨hal-01209325⟩
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ref_biblio: Guillaume Laurent, Christian Bonhomme, F. Babonneau. Solid-state nuclear magnetic resonance : from physics to materials. 3rd summer school of nanosciences in Ile-de-France, Jun 2009, Le Tremblay sur Mauldre, France. ⟨hal-01881873⟩
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ref_biblio: Cristina Coelho, Guillaume Laurent, Christian Bonhomme. Low Temperature NMR Study of Silicophosphate Materials. 9ème réunion de travail RMN du solide d’Eveux, Nov 2006, La Baume, France. ⟨hal-01881898⟩
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ref_biblio: Guillaume Laurent, Niki Baccile, Jocelyne Maquet, Christian Bonhomme, Florence Babonneau. Mesostructured silica studied by silicon filtered reverse cross-polarization solid state NMR. International school on high-field NMR spectroscopy for solids and liquids, May 2006, Les Houches, France. ⟨hal-01881960⟩
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